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Online Edition: "Specifications for Flavourings"
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Analytical Methods (Volume 4)
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Flavouring
N-[(Ethoxycarbonyl)methyl)-p-menthane-3-carboxamide
Synonym(s)
[1R-(1alpha,2beta,5alpha)]-N-[5-Methyl-2-(1-methylethyl)cyclohexyl]carbonyl glycine ethyl ester
Latest JECFA evaluation
2007 (Session 68)
Status of specification
Full
Information required
Chemical name
N-[(Ethoxycarbonyl)methyl)-p-menthane-3-carboxamide
JECFA number
1776
CAS number
68489-14-5
FEMA number
4309
COE number
FLAVIS number
Molecular weight
269.38
Chemical formula
C15H27NO3
Physical form/odour
White crystals or powder; Cool menthol aroma
Solubility
Practically insoluble or insoluble in water; slightly soluble in heptane; very slightly soluble in propylene glycol and ethyl acetate
Solubility in ethanol
Soluble
Boiling point (°C)
151° (2 mm Hg)
Assay min %
99%
Acid value max
Refractive index
NA
Specific gravity
NA
Other requirements
mp = 80-82°
ID Test
CNMR HNMR IR MS
Spectrum